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Fig. 2. XRD patterns of samples calcined at 600 °C for 6 h:

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Figure 8: XRD patterns of the microspherical samples calcined in N2 for 2 h at a) 800 °C, b) 900 °C, and c) 1000 °C

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Figure 3: Crystallite size for the as-synthesized and calcined samples (no combustion aid). Figure 3: Crystallite size for the as-synthesized and calc

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